Analysis of 6 volatile phenols in water samples by SPME-GC-FID

Analysis of 6 volatile phenols in water samples by SPME-GC-FID

Qingdao Zhenzheng Analytical Instrument Co., LTD. Technical department

SPMEProbe item number：ZZ-SPME-06-s

Analysis condition:

Sample: 10 ml water sample with standard, the concentration of volatile phenol was 20 ng/ml

Extraction temperature: 50 ºC; Extraction time: 30 min; Mixing speed: 600 rpm; Salt concentration: 30%, w:v; The pH value is 1

Desorption time: 3 min; Desorption temperature 250 ºC

Column: HP-1 30 m × 0.32 mm × 0.4 µm

Inlet: 250 ºC, no shunt injection;

Carrier gas: Nitrogen, flow rate 2.5 ml/min

Programmed temperature rise: 50 ºC for 2 min, 8 ºC/min to 100 ºC, 15 ºC/min to 250 ºC for 3 min

Detector: FID

GC-FID chromatogram

Linear range, linear correlation coefficient, minimum detection limit and repeatability

Test result of actual water sample and recovery rate of added standard